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Synthesis, Crystal Structure and Antitumor Activity of a New 3H-Phenanthro-[2,1-d]imidazol


3 4卷 9 期  2 01 5 . 9   结 构 化 学  J l E GoU  HUAXUE   V o 1 . 3 4 , No . 9   l 4 4 0 -1 4 4 5   Ch i n e s e  J .  S t r u c t .   Ch e m.   S y n t h e s i s , Cr y s t a l   S t r u c t u r e   a n d   An t i t u mo r   Ac t i v i t y   o f   a   Ne w  3 H- Ph e n a n t h r o . .   【 2 , 1 一 d ] i mi d a z o l e   De r i v a t i v e   0 f   De h y d r 0 a b i e t i c   Ac i d  ̄   GU  We n  ̄ MI AO  T i n gT i n g   . . WANG  S h i . . F a   J I N  Xi a o - - Ya n   HAO  Yu n   ZHANG  Ka n g ? - Pi n g   ( J i a n g s u K e y L a b   o f B i o m a s s - b a s e d G r e e n F u e l s a n dC h e m i c a l s , C o l l e g e o f   C h e mi c a l E n g i n e e r i n g , Na n j i n gF o r e s t r y   U n i v e r s i t y , N a n j i n g2 1 0 0 3 7 , C h i n a )   AB S T R ACT   T h e   t i t l e   c o mp o u n d( C I 9 H2 4 B r N3 0 2 , 3 ) wa s   s y n t h e s i z e d   f r o m  d e h y d r o a b i e t i c   a c i d   a n d   i t s   c r y s t a l   s t r u c t u r e   wa s   d e t e r mi n e d   b y   s i n g l e — c ys r t a l   X— r a y   d i f r a c t i o n . Th e   c o mp o u n d   i s   o f   mo n o c l i n i c   s y s t e m, s p a c e   g r o u p   C 2   wi t h   a   2 4 . 8 3 0 ( 5 ) , b=7 . 1 4 1 0 ( 1 4 ) , c= 1 3 . 9 8 1 ( 3 )A,   :   1 0 7 . 6 8 ( 3 ) 。 , Z  4 , V  2 3 6 1 . 9 ( 8 ) A   , Mr :4 8 2 . 4 2 , D。 =1 . 3 5 7   Mg / m’ , S= 1 . 0 0 3,   =1 . 7 7 2   mm~ ,   Y ( 0 0 0 ) =1 0 0 8 , t h e   i f n a l   R=0 . 0 6 6 0   a n d   w R=0 . 1 4 0 2   f o r

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